Description
Pharmaceutical Analysis 1 Notes B Pharmacy
Unit 1
Pharmaceutical Analysis
- Definition and scope of pharmaceutical analysis
- Different techniques of analysis
- Methods of expressing concentration with formula
- Primary and secondary standards
- Preparation and standardization of various molar and normal solutions
Error
- Errors in Analytical Chemistry
- Accuracy and Precision
- Significant figures
Topic
- Pharmacopoeia
- Impurities in pharmaceutical substances
- Limit test
Unit 2
Acid Base Titration
- Theories of acid base indicators
- Classification of acid base titrations
- Neutralization curves
Non-Aqueous Titration
- Introduction: Non-aqueous titration
- Solvents
- Acidimetry and alkalimetry titration
- Estimation of Sodium Benzoate:
- Estimation of Ephedrine HCl
Unit 3
Precipitation titrations
- Precipitation titrations
- Mohr’s method
- Volhard’s method
- Modified Volhard’s Method (Direct Volhard’s Method)
- Fajans Method (Adsorption Indicator Method)
- Estimation of sodium chloride
Complexometric titration
- Complexometric Titration
- Classification of Complexometric Titrations
- Metal ion indicators
- Masking and demasking reagents
- Estimation of Magnesium Sulfate by Complexometric Titration
- Estimation of Calcium Gluconate by Complexometric Titration
Gravimetry
- Gravimetric Analysis: Principle and Steps
- Purity of the precipitate: co-precipitation and post precipitation
- Estimation of Barium Sulfate (BaSOâ‚„) by Gravimetric Analysis
Diazotization titration
- Diazotization titration
Unit 4
Redox Titrations
- Introduction to Redox Titrations
- Concept of Oxidation
- Concept of Reduction
- Types of redox titrations
Unit 5
Conductometry
- Introduction to Conductometry in Pharmaceutical Analysis
- Conductivity Cell
- Conductometric Titrations
- Potentiometry
Potentiometry
- Electrochemical cell
- Reference Electrodes: Construction and Working
- Indicator Electrodes: Construction and Working
- Methods to Determine End Point in Potentiometric Titrations
Polarography
- Polarography
- Dropping Mercury Electrode (DME)
- Rotating Platinum Electrode (RPE)
- Applications of Polarography
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